英语翻译本实验采用液相反应法,称取1g上述制备的CMCTS置于10mLDMF中分散,并加入0.8g5-FuOH,在加入0.1gDMAp,在冰浴下缓慢滴加用10mL溶解的DCC,搅拌1小时后转至室温,搅拌反应24h.反应停止后,过滤,在

Question

英语翻译
本实验采用液相反应法,称取1g上述制备的CMCTS置于10mLDMF中分散,并加入0.8g 5-FuOH,在加入0.1g DMAp,在冰浴下缓慢滴加用10mL溶解的DCC,搅拌1小时后转至室温,搅拌反应24h.反应停止后,过滤,在固体物中依次加入适量的DMF、无水乙醇洗涤数次,干燥得产物.

Answer 1

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The said experiment adopts Liquid phase reaction method.Weigh 1g of prepared CMCTS and put into 10ml to disperse.Add 0.8g5-FuOH and 0.1g DMAp.Under ice bath,slowly dip 10ml of dissolving DCC.Stir one hour and trancfer to room temperature,stirring acting for 24hs.After reaction stopped,filter and add suitable DMF,absolute ethyl alcohol to be washed.Dry to get products.